Abstract

Methyl (2E)-3-methoxyacrylate and excess methylhydrazine yield crude 1- methyl-2-pyrazolin-5-one which is reacted with cyclohexanone to obtain the title compound in 86% yield. Detailed spectroscopic data (1H NMR, 13C NMR, 15N NMR, and MS) are presented.

Details

Title
Synthesis of 4,4'-(Cyclohexane-1,1-diyl)bis(1-methyl- 1H-pyrazol-5-ol)
Author
Eller, Gernot A; Holzer, Wolfgang
Pages
M569
Publication year
2008
Publication date
2008
Publisher
MDPI AG
e-ISSN
14228599
Source type
Scholarly Journal
Language of publication
English
ProQuest document ID
1530423300
Copyright
Copyright MDPI AG 2008