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Abstract

Conjugated donor–acceptor (D-A) copolymers are widely used in optoelectronic devices due to their influence on the resulting properties. This study focuses on the synthesis and characterization of the conjugated D-A copolymer constructed with fluorene and di-2-thienyl-2,1,3-benzothiadiazole units, resulting in Poly[2,7-(9,9-dioctyl-fluorene)-alt-5,5-(4,7-di(2-thienyl)-2,1,3-benzothiadiazole)] (PFDTBT). The synthesis associated with reaction times of 48 and 24 h, the latter incorporating the phase-transfer catalyst Aliquat 336, was investigated. The modified conditions produced copolymers with higher molar masses (Mw > 20,000 g/mol), improved thermal stability and red emission at 649 nm. Furthermore, the resulting D-A copolymers exhibited uniform morphology with low surface roughness (P2—Ra: 0.77 nm). These improved properties highlight the potential of D-A copolymers based on PFDTBT for various optoelectronic applications, including photovoltaics, light-emitting devices, transistors and biological markers in the form of quantum dots.

Details

1009240
Title
Synthesis and Characterization of Copolymers with Fluorene-di-2-thienyl-2,1,3-benzothiadiazole Units for Application in Optoelectronic Devices
Author
Barbosa de Brito, Elisa 1   VIAFID ORCID Logo  ; Daniela Corrêa Santos 2   VIAFID ORCID Logo  ; Taihana Parente de Paula 2 ; de Morais, Andreia 3 ; Jilian Nei de Freitas 3 ; Maria de Fátima Vieira Marques 2   VIAFID ORCID Logo  ; Sergio Neves Monteiro 4   VIAFID ORCID Logo 

 Center for Information Technology Renato Archer, (CTI Renato Archer), Rodovia D. Pedro I, Km 143, 6, Campinas 13069-901, SP, Brazil; Instituto de Macromoleculas Professora Eloisa Mano, IMA, Universidade Federal do Rio de Janeiro, IMA—UFRJ, Av. Horacio Macedo 2030, Rio de Janeiro 21941-598, RJ, Brazil 
 Instituto de Macromoleculas Professora Eloisa Mano, IMA, Universidade Federal do Rio de Janeiro, IMA—UFRJ, Av. Horacio Macedo 2030, Rio de Janeiro 21941-598, RJ, Brazil 
 Center for Information Technology Renato Archer, (CTI Renato Archer), Rodovia D. Pedro I, Km 143, 6, Campinas 13069-901, SP, Brazil 
 Military Institute of Engineering—IME, Department of Materials Science, Praça General Tibúrcio, 80, Urca, Rio de Janeiro 22290-270, RJ, Brazil 
Publication title
Polymers; Basel
Volume
17
Issue
1
First page
72
Publication year
2025
Publication date
2025
Publisher
MDPI AG
Place of publication
Basel
Country of publication
Switzerland
e-ISSN
20734360
Source type
Scholarly Journal
Language of publication
English
Document type
Journal Article
Publication history
 
 
Online publication date
2024-12-30
Milestone dates
2024-10-07 (Received); 2024-12-27 (Accepted)
Publication history
 
 
   First posting date
30 Dec 2024
ProQuest document ID
3153584926
Document URL
https://www.proquest.com/scholarly-journals/synthesis-characterization-copolymers-with/docview/3153584926/se-2?accountid=208611
Copyright
© 2024 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.
Last updated
2025-01-10
Database
2 databases
  • ProQuest One Academic
  • ProQuest One Academic