Content area

Abstract

Serial crystallography (SX) enables the determination of biologically relevant structures at room temperature while minimizing radiation damage. During SX experiments, the beam center on diffraction images can shift due to X-ray beam movements or detector displacement. Consequently, the geometry file for the beam center is optimized; however, the effects of deviations from the optimal position on data processing efficiency remain unclear. This study examines how changes in the beam center influence data quality by analyzing the indexing efficiency and structure refinement of lysozyme and glucose isomerase datasets, considering shifts in the beam center parameter. The results revealed that as the beam center deviated farther from its optimal position, the indexing efficiency declined, with the extent of the effect varying significantly across indexing algorithms. XDS and MOSFLM algorithms maintained high indexing efficiencies (>90%) for shifts of ≤4 pixels (688 μm) and ≤2 pixels (344 μm), respectively, compared to data processed at the optimized beam center. Conversely, the DirAx and XGANDALF algorithms exhibited indexing efficiencies below 90% for a two-pixel shift in the beam center. These findings enhance our understanding of how beam center shifts affect SX data processing and provide valuable insights for developing effective data processing strategies.

Details

1009240
Title
Effects of Beam Center Position Shifts on Data Processing in Serial Crystallography
Author
Publication title
Crystals; Basel
Volume
15
Issue
2
First page
185
Publication year
2025
Publication date
2025
Publisher
MDPI AG
Place of publication
Basel
Country of publication
Switzerland
Publication subject
e-ISSN
20734352
Source type
Scholarly Journal
Language of publication
English
Document type
Journal Article
Publication history
 
 
Online publication date
2025-02-15
Milestone dates
2025-01-20 (Received); 2025-02-14 (Accepted)
Publication history
 
 
   First posting date
15 Feb 2025
ProQuest document ID
3171020640
Document URL
https://www.proquest.com/scholarly-journals/effects-beam-center-position-shifts-on-data/docview/3171020640/se-2?accountid=208611
Copyright
© 2025 by the author. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.
Last updated
2025-02-26
Database
ProQuest One Academic