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Although Mercury Intrusion Porosimetry (MIP) and Nuclear Magnetic Resonance (NMR) are widely used for pore characterization, their effectiveness is fundamentally constrained by theoretical limitations. This study investigated the pore structure characteristics of coal-bearing sandstones from the northeastern Ordos Basin using an integrated approach combining experimental measurements and model-based inversion. The experimental measurements comprised a stress-dependent acoustic velocity test (P- and S-wave velocities), X-ray diffraction (XRD) mineralogical analysis, and NMR relaxation T2 spectra characterization. For model-based inversion, we developed an improved Mori-Tanaka (M-T) theoretical framework incorporating stress-sensitive pore geometry parameters and dual-porosity (stiff/soft) microstructure representation. Systematic analysis revealed four key findings: (1) excellent agreement between model-inverted and NMR-derived total porosity, with a maximum absolute error of 1.09%; (2) strong correlation between soft porosity and the third peak of T2 relaxation spectra; (3) stiff porosity governed by brittle mineral content (quartz and calcite), while soft porosity showing significant correlation with clay mineral abundance and Poisson’s ratio; and (4) markedly lower elastic moduli (28.78%–51.85%) in Zhiluo Formation sandstone compared to Yan’an Formation equivalents, resulting from differential diagenetic alteration despite comparable depositional settings. The proposed methodology advances conventional NMR analysis by simultaneously quantifying both pore geometry parameters (e.g., aspect ratios) and the stiff-to-soft pore distribution spectra. This established framework provides a robust characterization of the pore architecture in Jurassic sandstones, yielding deeper insights into sandstone pore evolution within the Ordos Basin. These findings provide actionable insights for water hazard mitigation and geological CO2 storage practices.
Details
Parameters;
Calcite;
S waves;
Clay minerals;
X-ray diffraction;
Wave velocity;
Sandstone;
Carbon dioxide;
Structural analysis;
P waves;
Nuclear magnetic resonance--NMR;
Porosity;
Microstructure;
Velocity;
Wave diffraction;
Modulus of elasticity;
Experiments;
Poisson's ratio;
Jurassic;
S-waves;
Acoustic velocity;
Coal mining;
Spectra;
Parameter sensitivity;
Aspect ratio;
Lithology;
Mineralogy;
Aquifers;
Geology;
Research methodology;
Hazard mitigation;
Physics;
Sedimentary rocks;
Permeability;
Diagenesis;
Nuclear magnetic resonance;
Acoustics;
Carbon capture and storage
; Li, Yueyue 2 ; Xu Haicheng 1
; Li, Wan 1 1 School of Resource and Earth Science, China University of Mining and Technology, Xuzhou 221116, China; [email protected] (H.Y.); [email protected] (H.X.); [email protected] (W.L.)
2 Inner Mongolia Huangtaolegai Coal Co., Ltd., Ordos 017000, China