Content area
The structural integrity of adhesively bonded composites is critically dependent on manufacturing process fidelity. While the MGS L418 epoxy system is widely used in aerospace applications, a quantitative hierarchy of its process variables is absent from the literature, leading to reliance on qualitative guidelines and inherent performance variability. This study closes this gap through a comprehensive sensitivity analysis. A 26-2 fractional factorial Design of Experiments (DOE) quantified the effects of six variables on single-lap shear strength. An Analysis of Variance (ANOVA) established a definitive hierarchy: induction time was the dominant factor, with a sub-optimal 15 min period causing a 74% strength reduction (p < 0.000). Surface preparation was the second most significant factor, with mechanical abrasion increasing strength by 17% (p = 0.000). Ambient humidity was a marginal factor (p = 0.013), linked to amine blush formation. The interaction effects were statistically insignificant, simplifying the control strategy. This work provides a validated, quantitative model that defines a robust process window, prioritizing induction time and surface preparation to de-risk manufacturing and ensure the reliability of safety-critical bonded structures.
Details
Fractional factorial design;
Shear tests;
Humidity;
Design of experiments;
Viscosity;
Shear strength;
Failure analysis;
Sensitivity analysis;
Structural integrity;
Process controls;
Bond strength;
Adhesives;
Manufacturing;
Variance analysis;
Safety critical;
Composite materials;
Adhesive bonding;
Surface preparation
1 Colegio Nueva Vizcaya, Investigation, Chihuahua 30809, Mexico; [email protected]; Tel.: +1-316-570-2012, Instituto Tecnologico de Chihuahua, Investigation, Chihuahua 30809, Mexico