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Abstract
An efficient condition for the microwave synthesis of nitroalkanes from α,β-unsaturated nitroalkenes using tri-n-butyltin hydride as a mild reducing reagent under aqueous conditions is described. A variety of conjugated nitroalkenes have undergone reduction chemoselectively to yield corresponding nitroalkanes up to 95% yield in 8–30 min. Also, a possible ionic mechanism involving a six-membered cyclic transition state has been proposed.
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Details
1 Department of Drug Design, University of Groningen, Antonius Deusinglaan 1, Postbus 196, Groningen 9700 AD, The Netherlands; Department of Organic Chemistry, Indian Institute of Science, Bangalore 560 012, India