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Abstract
Calamondin (Citrus microcarpa) essential oil is applied in different fields, including medicine, food, and cosmetic. This study aimed to determine theextraction yield of essential oil from Calamondin peels and optimize the extraction process using Response Surface Methodology (RSM). A three-level three-factors Box Behnken design with three variables including extraction temperature (103-137°C), time (95-145 min), and water to the material ratio (1.32-4.68 mL/g) was adopted. The aforementioned factors are identified to exert significant influence on the essential oil efficiency. Adopting a central composite design, optimal processing conditions were determined. The maximum yield of essential oil was 3.2%, achieved at conditions of the ratio of water and raw materials (3.20:1 mL/g), the temperature of 120.84°C and time of 21.27 min. The results showed good fits with the proposed model for the essential oil extraction (R2 = 99.71%).
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Details
1 NTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam; Faculty of Chemical Engineering and Food Technology, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam
2 NTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City, Vietnam
3 Department of Chemical Engineering, HCMC University of Technology, VNU-HCM, Ho Chi Minh City, Vietnam
4 Graduate University of Science and Technology, Vietnam Academy of Science and Technology, Ha Noi, Vietnam; Institute of Natural Products Chemistry, Vietnam Academy of Science and Technology, Ha Noi, Vietnam
5 Institute of Applied Materials Science, Vietnam Academy of Science and Technology, 01 TL29, District 12, Ho Chi Minh City, Vietnam