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Abstract
One kind of thermally reversible cross-linking agents for improving PVC thermally stability was synthesized. The chemical structure and thermally reversible characteristics of cross-linking agents were investigated by FTIR and DSC analysis, respectively. FTIR results confirmed that the cyclopentadienyl barium mercaptides ((CPD-C2H4S)2Ba) were successfully synthesized. DSC results showed it has thermally reversible characteristics and the depolymerization temperature was between 170 °C and 205 °C. The effects of cross-linking reaction time on gel content of Poly(vinyl chloride) compounds was evaluated. The gel content value arrived at 42% after being cross-linked for 25 min at 180 C. The static thermally stability measurement proved that the thermally stability of PVC compounds was improved.
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Details
1 Liaoning Key Laboratory of Advanced Polymer Matrix Composites Manufacturing Technology, Faculty of Aerospace Engineering, Shenyang Aerospace University, Shenyang 110136, China
2 Shenyang Rui Da Machinery Export and Import co., Ltd, Shenyang, 110000, China
3 School of Textile & Material Engineering, Dalian Polytechnic University, Dalian 116034, China