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Abstract
Magnetic iron oxide nanoparticle clusters (mnpc) coated with organic stabilizers were investigated using scanning transmission x-ray microscopy (STXM). Simultaneous surface and bulk sensitive Fe L3 edge absorption spectra, obtained using a photomultiplier tube and a channeltron, were used to detect subtle changes in the oxidation state in the surface and bulk of Iron Oxide mnpc. The effectiveness of this mode of STXM operation is demonstrated for these nanoparticle clusters.
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Details
1 Synchrotron SOLEIL, L’Orme des Merisiers, Saint-Aubin - BP 48, F-91192 Gif-sur-Yvette cedex, FRANCE
2 BAM Federal Institute of Materials Research and Testing, 12200 Berlin, Germany