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Abstract
We have established a new type of experimental set-up utilizing a Paris-Edinburgh (PE) type large volume press with a dedicated sample cell assembly for simultaneous x-ray diffraction, electrical resistance, and temperature gradient measurements at the High-Pressure Collaborative Access Team (HPCAT) at Advanced Photon Source (APS), Argonne National Laboratory 16BM-B beamline. We demonstrate the feasibility of performing in situ measurements and correlating the measured electrical-thermal-structural properties over a broad range of P-T conditions by observing the well-known solid-solid and solid-melt transitions of bismuth (Bi) up to 5 GPa and 600° C. The goal of developing this new multi-probe measurement capability is to further improve detection of the onset of solid-solid and solid-melt transitions, relate structural and electrical properties of materials, determine changes in thermal conductivity at high P-T, and ultimately extend the technique for investigating other parameters, such as the Seebeck coefficient of thermoelectric materials.
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Details
1 HiPSEC, University of Nevada, Las Vegas. 4505 S. Maryland Parkway Las Vegas, NV 89154, USA; Shock and Detonation Physics Group, Los Alamos National Laboratory, Los Alamos, NM 87545, USA
2 HiPSEC, University of Nevada, Las Vegas. 4505 S. Maryland Parkway Las Vegas, NV 89154, USA
3 Shock and Detonation Physics Group, Los Alamos National Laboratory, Los Alamos, NM 87545, USA
4 HPCAT, Geophysical Laboratory, Carnegie Institution of Washington, 9700 South Cass Ave., 434E, Argonne, IL 60439, USA