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Abstract
A new co-crystal explosive of 1,3,5,7-tetranitro-1,3,5,7-tetrazocane (HMX) and 3-nitro-1, 2, 4-triazol-5-one (NTO) in a molar ratio of 1:1 has been prepared by solvent/anti-solvent method. The SEM photographs show that HMX/NTO co-crystals are distinctly different from HMX and NTO crystals. The co-crystals are prisms with well formed crystal surfaces. Thermal analysis results indicate the melting point of the co-crystal is 29.3 °Chigher than that of NTO. Moreover, the co-crystal exhibits a modified mechanical sensitivity. The characteristic height (H50) of impact sensitivity increases 14.8cm, and the explosion percentage (P) of friction sensitivity decreases by 40% compared with HMX. The HMX/NTO co-crystals possess good thermal property and low sensitivity, which mean huge advantages in blasting engineering.
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Details
1 Institute of Chemical Defence, P.O. Box 1048, Beijing 102205, China; State key laboratory of NBC Protection for Civilian, Research Institute of Chemical Defence, Beijing 102205, China
2 National key laboratory of explosive science and technology, Beijing Institute of Technology, Beijing 100081, China
3 State key laboratory of NBC Protection for Civilian, Research Institute of Chemical Defence, Beijing 102205, China
4 Institute of Chemical Defence, P.O. Box 1048, Beijing 102205, China